ASTM D1160 Vacuum Distillation Apparatus
What ASTM D1160 (ISO 6616) measures, how it differs from D2892 crude TBP, and what a turn-key vacuum apparatus includes.
ReadNotes on distillation, solvent recycling, crude oil analysis, and laboratory equipment.
What ASTM D1160 (ISO 6616) measures, how it differs from D2892 crude TBP, and what a turn-key vacuum apparatus includes.
ReadBoiler, column, condenser, reflux, and receivers. How a complete lab system differs from kit glassware.
ReadWhen to choose a spinning band column versus a packed column for laboratory fractional distillation. Efficiency, hold-up, and throughput...
ReadHow to size B/R fractional distillation systems: micro, mini, lab scale 9600, and pilot, based on sample volume...
ReadTheoretical plates vs hold-up: how column efficiency and inventory affect purity and yield in laboratory fractional distillation...
ReadB/R 9600 lab scale fractional distillation: multi-liter flasks, column options, automation, and typical applications...
ReadHow spinning band distillation helps purify specialty chemicals and natural products when efficiency and low hold-up both matter...
ReadCould your lab continue operating if alcohol, xylene, or formalin suddenly became difficult to get? How onsite solvent recycling builds resilience against supply chain disruption...
ReadB/R Instrument recognizes and thanks Richard Roark, Sr. for his lifetime of dedication, leadership, and service as President and CEO. Matt Baer, a 10-year veteran of B/R Instrument, becomes President effective June 1, 2026...
ReadA Cadiot Distillation Column is also known as a Spinning Band distillation column. One application of Cadiot distillation is for wine analysis, specifically...
ReadIf you have 5 minutes a day, you have enough time to recycle your solvents. That may sound like an exaggeration but recycling doesn't take much time. A B/R...
ReadThe recycled purity can depend a lot on the recycler being used. With a B/R recycler you can expect high purity recycled solvents. The table below shows...
ReadQ: Our lab is already crowded. Does a recycler take up much space? Space is always in short supply. Choose a "space efficient" recycler and you are on your way...
ReadBy now you've heard that many histology labs are recycling their xylene, alcohol, and formalin. What are some reasons to recycle solvents? Don't Throw Solvents...
ReadQ: My old recycler needed water and a drain. Do today's recyclers need a water hook up? No, you don't need a water hook up or drain. Older solvent recyclers...
ReadA B/R recycler can recycle a solvent forever! Solvents used for tissue processing or staining becomes contaminated with stain, water, fat, protein, wax, and...
ReadDo filter-based recyclers work? The answer is both yes and no, but mostly no. There are commercial filter recyclers available for alcohol and formalin....
ReadQ: Our lab wants to switch to xylene substitutes. Can they be recycled? Actually, xylene substitutes are easier to recycle than xylene. Their higher boiling...
ReadQ: How many years will a solvent recycler last before it needs replacing? 10 to 15 years or...Longer. Do you remember your cell phone from 15 years ago? The...
ReadNo, B/R recyclers do not require special ventilation or a special room. B/R Solvent recyclers are closed systems - no special ventilation needed. B/R solvent...
ReadQ: My boss wants our lab to start recycling solvents. How do I know if it makes financial sense? Solvent recycling saves money! That's the main driving force...
ReadQ: How do I fill my recycler? Most recyclers have more than one way to fill them. You can choose the fill method that fits your lab. Direct fill - One pour and...
ReadQ: How do I know my recycled solvents are pure? You can use the following quick tests to check the purity of the recycled solvents. Xylene: The Graduated...
ReadQ: I've heard some recycled solvents smell fishy. Is there a way to avoid that? Bad smelling solvent is an unpleasant problem but it's easy to avoid. Waste...
ReadQ: If I am recycling more than one solvent in a recycler, how do I avoid cross contamination between the solvents? After making your solvents nice and clean in...
ReadSolvent recycling in our lab? Sounds great but can't somebody else do it for us? A growing trend in hospitals is for Environmental Health and Safety (EH&S) to...
ReadWith a 20 liter (5 gallon) recycler you can easily recycler 5000 to 10000 liters (1300 to 2700 gallons) of solvent in a year. Typical operating costs to...
ReadIf you need consistent, high-quality recycled solvents, you need fractional distillation. Fractional distillation is a technique used to purify solvents,...
ReadAll About Alcohol Recycling You've been using alcohol for years and are thinking about recycling it. That is a great idea that will save you money! It doesn't...
ReadHow Does Formalin Recycling Work? You've been using formalin for years and are thinking about recycling it. That's a great idea that will save you money! While...
ReadLabs spend significant sums on buying and disposing of histology solvents. Unseen to most, are the regulatory costs of complying with local and federal...
ReadTell me about the details of the xylene recycling process Note: With regard to solvent recycling xylene and xylene substitutes are nearly interchangeable. In...
ReadVery small amounts of crude oil (7 - 100 ml) can be distilled with the B/R micro crude oil distillation system. The spinning band with a maximum of 15...
ReadDistilling small samples of crude oil 100- 1000 ml Distilling small samples of crude oil can be a challenge. The "hold up" in the column packing...
ReadReflux is the return of condensed distillation vapor to the boiling flask. Reflux ratio is the ratio of the condensate returned to the boiling flask to the...
ReadCondensate is a by product of raw natural gas composed of light hydrocarbons which can be condensed when below their dew point. There are 3 primary sources of...
ReadHigh levels of water in crude oil make fractional distillation difficult. Water has a hard time vaporizing from the boiling flask and getting through the...
ReadTrue boiling point distillation distills crude oil from the initial boiling point up to 370-400 °C. D2892 is the ASTM test number. It is most commonly used to...
ReadNot all Crude Oil is the Same. How can you do Quality Control? Refineries buy large volumes of crude oil. But when a 500,000 barrel tanker arrives, how do they...
ReadRead on to learn more about butane collection for true boiling point distillation. Butane is a component of crude oil that boils well below room temperature....
ReadVacuum Pot Still (VPS) The vacuum pot still distills crude oil residue from 370 ºC up to 565 ºC. D5236 is the ASTM test number. It is most commonly used to...
ReadLab-scale Crude Oil Distillation Distillation of crude oil in the laboratory models what happens in the refinery. The results of the lab-scale distillation...
ReadTrue boiling point distillation has distillation column packing that has 15 theoretical plates of efficiency. Many different types of packing are currently...
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