B/R Instrument blog

Notes on distillation, solvent recycling, crude oil analysis, and laboratory equipment.

Crude Oil Distillation · Aug 14, 2026

ASTM D1160 Vacuum Distillation Apparatus

What ASTM D1160 (ISO 6616) measures, how it differs from D2892 crude TBP, and what a turn-key vacuum apparatus includes.

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Fractional Distillation · Aug 5, 2026

How a Fractional Distillation Column Works

Boiler, column, condenser, reflux, and receivers. How a complete lab system differs from kit glassware.

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Fractional Distillation · Jul 22, 2026

Spinning Band vs Packed Column Distillation

When to choose a spinning band column versus a packed column for laboratory fractional distillation. Efficiency, hold-up, and throughput...

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Fractional Distillation · Jul 8, 2026

Choosing Micro, Mini, Lab Scale, or Pilot Distillation

How to size B/R fractional distillation systems: micro, mini, lab scale 9600, and pilot, based on sample volume...

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Fractional Distillation · Jun 17, 2026

Theoretical Plates and Hold-up in Laboratory Distillation

Theoretical plates vs hold-up: how column efficiency and inventory affect purity and yield in laboratory fractional distillation...

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Fractional Distillation · May 28, 2026

Lab Scale Fractional Distillation Systems (9600 Overview)

B/R 9600 lab scale fractional distillation: multi-liter flasks, column options, automation, and typical applications...

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Fractional Distillation · May 6, 2026

Spinning Band Distillation for Specialty Chemicals and Natural Products

How spinning band distillation helps purify specialty chemicals and natural products when efficiency and low hold-up both matter...

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Solvent Recycling · Jul 31, 2026

The Unexpected Risk Facing Histology and Pathology Labs

Could your lab continue operating if alcohol, xylene, or formalin suddenly became difficult to get? How onsite solvent recycling builds resilience against supply chain disruption...

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News · Jun 10, 2026

B/R Instrument Honors Richard Roark, Sr. for a Lifetime of Leadership and Service

B/R Instrument recognizes and thanks Richard Roark, Sr. for his lifetime of dedication, leadership, and service as President and CEO. Matt Baer, a 10-year veteran of B/R Instrument, becomes President effective June 1, 2026...

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Fractional Distillation · Apr 21, 2020

Cadiot Distillation for Wine Analysis

A Cadiot Distillation Column is also known as a Spinning Band distillation column. One application of Cadiot distillation is for wine analysis, specifically...

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Solvent Recycling · Jul 22, 2019

Is Solvent Recycling A Lot Of Work?

If you have 5 minutes a day, you have enough time to recycle your solvents. That may sound like an exaggeration but recycling doesn't take much time. A B/R...

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Solvent Recycling · Jul 21, 2019

How Pure Are Recycled Solvents?

The recycled purity can depend a lot on the recycler being used. With a B/R recycler you can expect high purity recycled solvents. The table below shows...

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Solvent Recycling · Jul 20, 2019

How Much Space Does A Solvent Recycler Take Up?

Q: Our lab is already crowded. Does a recycler take up much space? Space is always in short supply. Choose a "space efficient" recycler and you are on your way...

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Solvent Recycling · Jul 19, 2019

5 Reasons To Recycle Solvents

By now you've heard that many histology labs are recycling their xylene, alcohol, and formalin. What are some reasons to recycle solvents? Don't Throw Solvents...

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Solvent Recycling · Jul 18, 2019

What utilities do I need to operate solvent recycling equipment?

Q: My old recycler needed water and a drain. Do today's recyclers need a water hook up? No, you don't need a water hook up or drain. Older solvent recyclers...

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Solvent Recycling · Jul 17, 2019

How many times can I recycle a solvent?

A B/R recycler can recycle a solvent forever! Solvents used for tissue processing or staining becomes contaminated with stain, water, fat, protein, wax, and...

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Solvent Recycling · Jul 16, 2019

Do filter based solvent recyclers work?

Do filter-based recyclers work? The answer is both yes and no, but mostly no. There are commercial filter recyclers available for alcohol and formalin....

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Solvent Recycling · Jul 15, 2019

Can I recycle xylene substitutes?

Q: Our lab wants to switch to xylene substitutes. Can they be recycled? Actually, xylene substitutes are easier to recycle than xylene. Their higher boiling...

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Solvent Recycling · Jul 14, 2019

How long does a Solvent Recycler last?

Q: How many years will a solvent recycler last before it needs replacing? 10 to 15 years or...Longer. Do you remember your cell phone from 15 years ago? The...

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Solvent Recycling · Jul 13, 2019

Does a solvent recycler need ventilation?

No, B/R recyclers do not require special ventilation or a special room. B/R Solvent recyclers are closed systems - no special ventilation needed. B/R solvent...

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Solvent Recycling · Jul 12, 2019

Does Solvent Recycling Make Cents...Dollars?

Q: My boss wants our lab to start recycling solvents. How do I know if it makes financial sense? Solvent recycling saves money! That's the main driving force...

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Solvent Recycling · Jul 11, 2019

How do I fill my recycler?

Q: How do I fill my recycler? Most recyclers have more than one way to fill them. You can choose the fill method that fits your lab. Direct fill - One pour and...

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Solvent Recycling · Jul 10, 2019

Recycled Solvent Purity Test

Q: How do I know my recycled solvents are pure? You can use the following quick tests to check the purity of the recycled solvents. Xylene: The Graduated...

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Solvent Recycling · Jul 09, 2019

Should recycled solvents smell fishy?

Q: I've heard some recycled solvents smell fishy. Is there a way to avoid that? Bad smelling solvent is an unpleasant problem but it's easy to avoid. Waste...

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Solvent Recycling · Jul 08, 2019

No Rinse Cycle

Q: If I am recycling more than one solvent in a recycler, how do I avoid cross contamination between the solvents? After making your solvents nice and clean in...

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Solvent Recycling · Jul 07, 2019

Solvent recycling is great, especially if someone else does it for you

Solvent recycling in our lab? Sounds great but can't somebody else do it for us? A growing trend in hospitals is for Environmental Health and Safety (EH&S) to...

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Solvent Recycling · Jul 06, 2019

How much does it cost to operate a Solvent Recycler?

With a 20 liter (5 gallon) recycler you can easily recycler 5000 to 10000 liters (1300 to 2700 gallons) of solvent in a year. Typical operating costs to...

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Solvent Recycling · Jul 05, 2019

Fractional Distillation and Solvent Recycling

If you need consistent, high-quality recycled solvents, you need fractional distillation. Fractional distillation is a technique used to purify solvents,...

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Solvent Recycling · Jul 04, 2019

Alcohol Recycling 101

All About Alcohol Recycling You've been using alcohol for years and are thinking about recycling it. That is a great idea that will save you money! It doesn't...

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Solvent Recycling · Jul 03, 2019

Formalin Recycling 101

How Does Formalin Recycling Work? You've been using formalin for years and are thinking about recycling it. That's a great idea that will save you money! While...

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Solvent Recycling · Jul 02, 2019

Reduce your waste generator status and save a ton of paperwork

Labs spend significant sums on buying and disposing of histology solvents. Unseen to most, are the regulatory costs of complying with local and federal...

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Solvent Recycling · Jul 01, 2019

Xylene Recycling 101

Tell me about the details of the xylene recycling process Note: With regard to solvent recycling xylene and xylene substitutes are nearly interchangeable. In...

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Crude Oil Distillation · Dec 14, 2018

Micro Distillation of Crude Oil 7 to 100 ml

Very small amounts of crude oil (7 - 100 ml) can be distilled with the B/R micro crude oil distillation system. The spinning band with a maximum of 15...

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Crude Oil Distillation · Dec 14, 2018

Mini-Crude Oil Distillation

Distilling small samples of crude oil 100- 1000 ml Distilling small samples of crude oil can be a challenge. The "hold up" in the column packing...

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Crude Oil Distillation · Dec 09, 2018

Reflux Ratio and D2892 Crude Oil Distillation

Reflux is the return of condensed distillation vapor to the boiling flask. Reflux ratio is the ratio of the condensate returned to the boiling flask to the...

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Crude Oil Distillation · Dec 09, 2018

Condensate Distillation with D2892 crude oil distillation

Condensate is a by product of raw natural gas composed of light hydrocarbons which can be condensed when below their dew point.  There are 3 primary sources of...

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Crude Oil Distillation · Dec 09, 2018

Dehydration of Crude Oil - D2892 (De-watering)

High levels of water in crude oil make fractional distillation difficult. Water has a hard time vaporizing from the boiling flask and getting through the...

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Crude Oil Distillation · Nov 24, 2018

True Boiling Point Distillation - ASTM D2892 Distillation of Crude Oil

True boiling point distillation distills crude oil from the initial boiling point up to 370-400 °C. D2892 is the ASTM test number. It is most commonly used to...

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Crude Oil Distillation · Nov 20, 2018

Why Distill Crude Oil on a Lab Scale?

Not all Crude Oil is the Same. How can you do Quality Control? Refineries buy large volumes of crude oil. But when a 500,000 barrel tanker arrives, how do they...

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Crude Oil Distillation · Nov 19, 2018

Butane Collection for True Boiling Point Distillation - ASTM D2892

Read on to learn more about butane collection for true boiling point distillation. Butane is a component of crude oil that boils well below room temperature....

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Crude Oil Distillation · Nov 19, 2018

Vacuum Pot Still: ASTM D5236 for Distillation of Heavy Hydrocarbons

Vacuum Pot Still (VPS) The vacuum pot still distills crude oil residue from 370 ºC up to 565 ºC. D5236 is the ASTM test number. It is most commonly used to...

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Crude Oil Distillation · Nov 12, 2018

Modeling Refining with Lab-Scale Crude Oil Distillation: ASTM D2892

Lab-scale Crude Oil Distillation Distillation of crude oil in the laboratory models what happens in the refinery.  The results of the lab-scale distillation...

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Crude Oil Distillation · Nov 12, 2018

True Boiling Point (TBP) Distillation Column Packing: ASTM D2892 Crude Oil Distillation

True boiling point distillation has distillation column packing that has 15 theoretical plates of efficiency. Many different types of packing are currently...

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